Jiuerxin capsule
Product description of Aizhuerxin Capsule
(I) Product introduction
[Prescription] Panax notoginseng 134G Chuanxiong 335g Danshen 67g
Safflower 134g Alisma alisma 67g Acanthopanax senticosus plus extract powder 31g
[Method] The above six flavors, 37 crushed into fine powder, sieve;The volatile oil was extracted from ligusticum chuanxiong, and the distilled aqueous solution was collected by another device.Liquid and safflower, salvia miltiorrhiza, alisma, add water decoction twice, the first 3 hours, the second 2 hours, merging decoction, filtration, the filtrate and the distillation of aqueous solution to merge, condensed into concrete, drying, crushing, and notoginseng powder, acanthopanax extract powder blending, injection rhizoma ligustici wallichii volatile oil, blending, seal for 2 hours, encapsule, made 500 grains, quick.
[Properties] This product is capsule, the content is brownish yellow, fragrant, bitter, astringent after sweet.
(1) Take the content of this product about 0.5g, add 10ml ethanol, heat reflux for 30 minutes, cool, filter, take 2ml filtrate, add sodium nitrite solution (1 20) 0.3ml and 10% aluminum nitrate solution 0.3ml, shake well, place for 3 minutes, add sodium hydroxide solution (0.1mol/L) 2ml, that is, reddish brown.
(2) Take 1g of the content of this product, add petroleum ether (60~90℃) 10ml, soak for 6 hours, shake constantly, filter, take 1ml of filtrate, steam dry, residue add 1ml methanol to dissolve, add 2~3 drops of 2% nitrobenzoic acid methanol solution and 2 drops of potassium hydroxide saturated methanol solution, purple red.
(3) the contents about 2 g amount of this product, methanol 20 ml, dipping 30 minutes, all the vibration wave, filtration, the filtrate zhenggan 10 ml of water dissolution, filtration, the filtrate extracted with ether twice, each time 10 ml, abandon to ether liquid, reoccupy n-butyl alcohol extract three times, each time 5 ml, combination of n-butyl alcohol extract, boiled, add 1 ml methanol dissolved, greatly as the solution.Let's take 37 R1, methanol was added to prepare a solution containing 2.5mg per 1mL as the reference solution.According to thin layer chromatography (Page 57 of Appendix), 5μ L of the above two solutions were absorbed, respectively, on the same silica gel G thin layer plate, the upper solution of N-butanol-ethyl acetate water (4-1:5) was used as the developing agent, unfolded, dried, and sprayed with sulfuric acid solution (1 10), at 105℃ for about 10 minutes.In the chromatogram of the tested substance, spots of the same color appeared at the corresponding position of the chromatogram of the reference substance.
(4) take 0.5g of the content of the product, add anhydrous ethanol to reflux for 30 minutes, cool, filter, take 2ml of filtrate, put in a 25ml measuring cup, add anhydrous ethanol to the scale, spectrophotometry (appendix 51 page) determination, the maximum absorption at 281nm wavelength.
[Inspection] It should comply with the relevant provisions under the capsule item (Appendix 16 page).
[Functions and Indications] Invigorate blood circulation, remove blood stasis and give birth to new life.For coronary heart disease, gelatinous pain.
[Usage and Dosage] Take orally, 2-4 tablets at a time, 3 times a day.
[Specification] 0.45g per tablet.
Storage To seal.
Acanthopanax extractives powder is acanthopanax extractives (p. 458), dried and crushed.
[Precautions] This product is not suitable for blood deficiency without blood stasis, pregnant women should use with caution.
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